action commences, and the whole allowed to rest the
specified time.
Whilst saponification is proceeding, the "sugar solution" is prepared by
dissolving 50 lb. cane sugar in 50 lb. water, at 168 deg. F. (76 deg. C.), to
which may be added 5 lb. soda crystals, and any necessary colouring
matter. The water used for this solution should be as soft as possible,
as hard water is liable to produce opaque streaks of lime soap.
It is absolutely necessary before proceeding further to ensure that
saponification is complete. A greasy, soft feel and the presence of
"strength" (caustic) would denote incomplete saponification--this can
only be remedied by further heating and crutching. Deficiency of caustic
alkali should also be avoided, and, if more lye is required, great care
must be exercised in its addition.
Saponification being completed, the sugar solution is carefully and
gradually crutched into the soap; when the contents of the pan have
become a homogeneous and syrupy mass, the crutching is discontinued, and
the pan is covered for one hour. The heat of the soap in the pan should
not exceed 170 deg. F. (77 deg. C.).
Having rested the necessary period, the soap will have a slight froth on
the surface, but will be clear underneath and appear dark. Samples may
now be withdrawn, cooled, and examined prior to framing. If the process
has been successfully performed the soap will be firm and transparent,
of uniform colour, and possess only a faintly alkaline taste.
If the sample be firm but opaque, more sugar solution is required; this
should be added very carefully whilst crutching, an excess being
specially guarded against. If the sample be soft, although transparent,
and the alkaline taste not too pronounced, the soap evidently contains
an excess of water, which may be remedied by the addition of a small
quantity of soda ash; too much soda ash (carbonates) must be avoided,
lest it should produce efflorescence.
Having examined the soap and found it to be correct, or having remedied
its defects, the soap in the pan is allowed to cool to 145 deg. F. (63 deg. C.)
and perfume added. The soap is now quickly filled into narrow frames and
allowed to cool rapidly.
The blocks of soap should not be stripped until quite cold throughout,
and they should be allowed to stand open for a while before slabbing.
When freshly cut into tablets, the soap may appear somewhat turbid, but
the brightness comes with the exposure it will receiv
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