arency is sometimes assisted and hastened by
the addition of glycerine or a solution of cane-sugar.
A patent has been granted to A. Ruch (Fr. Pat. 327,293, 1902) for the
manufacture of transparent glycerine soap by heating in a closed vessel
fatty acids together with the requisite quantity of alcoholic caustic
soda solution necessary for saponification, and cooling the resultant
soap. It is also proposed to add sugar solution.
Cheaper qualities of transparent soaps are made by the cold process with
or without the aid of alcohol and castor oil, and with the assistance of
glycerine or cane-sugar.
With the continual demand for cheaper production, sugar solution has
gradually, in conjunction with castor oil, which produces transparency,
superseded the use of alcohol and glycerine.
For a small batch, 56 lb. Cochin cocoa-nut oil and 56 lb. sweet edible
tallow may be taken, melted at 130 deg. F. (54 deg. C.), and carefully strained
into a small steam-jacketed pan. It is imperative that the materials
should be of the highest quality and perfectly clean. Twenty-three lb.
of pure glycerine and 56 lb. of bright caustic soda solution made from
high grade caustic and having a density of 72 deg. Tw. (38 deg. B.) are crutched
into the fat; the alcohol, which would be 45 lb. in this example, is
then added. The whole must be most intimately incorporated, and the pan
covered and allowed to rest for one hour or one and a half hours.
Saponification should ensue.
To produce a transparent glycerine soap with the aid of castor oil, and
with or without the use of alcohol, the following is the procedure:--
Cochin cocoa-nut oil, sweet edible tallow, and castor oil, of each 56
lb. are taken, warmed to 130 deg. F. (54 deg. C.), and carefully strained into
the jacketed pan. If it is desired to use glycerine and cane sugar
solution, and no alcohol, the glycerine (25 lb.) is now stirred into the
fats together with the requisite (83 lb.) caustic soda solution 72 deg. Tw.
(38 deg. B.). If it is intended to use alcohol and sugar, and no glycerine,
the latter is replaced by 47 lb. of alcohol, and added after the
incorporation of the caustic soda lye.
The whole being thoroughly crutched, the pan is covered and
saponification allowed to proceed for one hour or one and a half hours.
Should the saponification for some reason be retarded, a little steam
may be very cautiously admitted to the jacket of the pan, the mass well
crutched until the re
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