FREE BOOKS

Author's List




PREV.   NEXT  
|<   46   47   48   49   50   51   52   53   54   55   56   57   58   59   60   61   62   63   64   65   66   67   68   69   70  
71   72   73   74   75   76   77   78   79   80   81   82   83   84   85   86   87   88   89   90   91   92   93   94   95   >>   >|  
imits of dilution and corresponding effect, the process allows of the production of either a 'bulk' or a 'condensed' powder. We prefer to use about five litres of the liquid to each one kilo. of grain operated upon, as this quantity allows of the grains being freely suspended in the liquid upon stirring. The grains are run into the liquid, which is then preferably heated to the boiling-point for a few minutes whilst the whole is gently stirred. Under this treatment the grains assume a more or less rounded gelatinous condition according to the strength of the liquid. There is, however, no solution of the guncotton and practically no tendency of the grains to cohere. Each grain, however, is acted upon _throughout_ and perfectly _equally_. After a few minutes' treatment, water is gradually added, when the grains rapidly harden. They are then freed from acetone and certain impurities by washing with water, heating, and drying. The process is of course carried out in a vessel provided with any means for gentle stirring and heating, and with an outlet for carrying off the volatilised solvent which is entirely recovered by condensation, the grains parting with the acetone with ease. _Stabilising cellulose nitrates._--The process is of especial value in rendering stable and inert the traces of unstable compounds which always remain in cellulose nitrate after the ordinary boiling and washing process. It is of greatest value in the manufacture of collodion cotton used for the preparation of gelatinous blasting explosives and all explosives composed of nitroglycerin and cellulose nitrates. Such mixtures seem peculiarly liable to decomposition if the cellulose nitrate is not of exceptional stability (J. Soc. Chem. Ind., 1899, 787). EMPLOI DE LA CELLULOSE POUR LA FABRICATION DE FILS BRILLANTS IMITANT LA SOIE. E. BRONNERT (1) (Rev. Mat. Col., 1900, September, 267). V. ~USE OF CELLULOSE IN THE MANUFACTURE OF IMITATIONS OF SILK (LUSTRA-CELLULOSE).~ (p. 45) _Introduction._--The problem of spinning a continuous thread of cellulose has received in later years several solutions. Mechanically all resolve themselves into the preparation of a structureless filtered solution of cellulose or a cellulose derivative, and forcing through capillary orifices into some medium which either absorbs or decomposes the solvent. The author notes here that the fineness and to a great extent the softness of the product depends upon the dimens
PREV.   NEXT  
|<   46   47   48   49   50   51   52   53   54   55   56   57   58   59   60   61   62   63   64   65   66   67   68   69   70  
71   72   73   74   75   76   77   78   79   80   81   82   83   84   85   86   87   88   89   90   91   92   93   94   95   >>   >|  



Top keywords:

cellulose

 

grains

 

liquid

 

process

 

CELLULOSE

 
stirring
 

boiling

 

gelatinous

 

solution

 

acetone


treatment
 

heating

 

washing

 

minutes

 

nitrate

 

preparation

 

solvent

 
explosives
 

nitrates

 

FABRICATION


blasting

 

BRILLANTS

 

BRONNERT

 

manufacture

 

cotton

 

collodion

 
IMITANT
 
liable
 

peculiarly

 
stability

decomposition

 

exceptional

 

EMPLOI

 
nitroglycerin
 

composed

 

mixtures

 

capillary

 

orifices

 
medium
 

forcing


derivative

 

resolve

 

structureless

 

filtered

 

absorbs

 

decomposes

 
softness
 
extent
 

product

 

depends