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Ferric oxalate solution 100 parts Neutral ammonium oxalate 18 to 20 parts B. SODIO-FERRIC OXALATE SOLUTION Ferric oxalate solution 100 parts Neutral sodium oxalate 15 to 18 parts To prepare these two solutions the ammonium or sodium oxalate is dissolved by small quantities at a time, and when the emerald color due to the formation of the double oxalate commences to darken, the saturation being then complete, no more of either salt should be added. The solution is now well shaken with 3 parts of glycerine, allowed to settle and filtered. Any one of the double oxalates can be used. The ammonium tends to produce softer pictures and bluish tones. To obtain more contrasts a little potassium chlorate may be added. C. IRON CHLORATE SOLUTION Solution B 100 parts Potassium chlorate 0.4 part D. MERCURIC SOLUTION. Mercuric chloride 20 parts solution at 5:100 Sodium oxalate solution 40 parts at 3:100 Glycerine 2 parts SENSITIZING SOLUTIONS. FOR BLACK TONES. Platinite solution, 1:6 5 parts Solution B 6 parts Solution C 2 parts FOR SEPIA TONES. Platinite solution, 1:6 5 parts Solution C 4 parts Solution D 4 parts Intermediate tones are obtained by diminishing the dose of C and replacing it by an equal volume of B. For this process the paper should be sized with Arrowroot 2 parts Sodium oxalate at 3:100 100 parts To dispense with this preliminary sizing Captain Pizzighelli adds gum arabic to the platinite solution, whereby the sizing and sensitizing are done in one operation. The gum arabic solutions are prepared as follows: E. Gum arabic in 40 parts powder Sodium ferric 40 parts oxalate solution, B Sodium oxalate 100 parts solution at 3:100 Glycerine 3 parts Place the glycerine and the gum arabic in a mortar, then, stirring with the pestle, dissolve by adding, little by little, the mixture, heated to 40--45 deg. C. (104--113 deg. Fahr.), of the solution of sodium ferric oxalate and sodium oxalate. Let stand for about two hours and grind again to dissolve entirely the gum arabic. Filter through muslin. F. Mercuric chloride 20 parts solution, 5:100 Sodium oxalate solution, 40 parts 3:100 Gum arabic in powder 24 parts Glycerine
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