lecting several precipitates
on the same filter, is a strong argument in favor of its use with any
but gelatinous precipitates.]
!Method B. With the Use of a Paper Filter!
PROCEDURE.--Weigh out two portions of sodium chloride of about
0.25-0.3 gram each and proceed with the precipitation of the silver
chloride as described under Method A above. When the chloride is ready
for filtration prepare two 9 cm. washed paper filters (see Appendix).
Pour the liquid above the precipitates through the filters, wash twice
by decantation and transfer the precipitates to the filters, finally
washing them until free from silver solution as described. The funnel
should then be covered with a moistened filter paper by stretching it
over the top and edges, to which it will adhere on drying. It should
be properly labeled with the student's name and desk number, and then
placed in a drying closet, at a temperature of about 100-110 deg.C., until
completely dry.
The perfectly dry filter is then opened over a circular piece of
clean, smooth, glazed paper about six inches in diameter, placed upon
a larger piece about twelve inches in diameter. The precipitate is
removed from the filter as completely as possible by rubbing the sides
gently together, or by scraping them cautiously with a feather which
has been cut close to the quill and is slightly stiff (Note 1). In
either case, care must be taken not to rub off any considerable
quantity of the paper, nor to lose silver chloride in the form of
dust. Cover the precipitate on the glazed paper with a watch-glass to
prevent loss of fine particles and to protect it from dust from the
air. Fold the filter paper carefully, roll it into a small cone, and
wind loosely around !the top! a piece of small platinum wire (Note 2).
Hold the filter by the wire over a small porcelain crucible (which has
been cleaned, ignited, cooled in a desiccator, and weighed), ignite
it, and allow the ash to fall into the crucible. Place the crucible
upon a clean clay triangle, on its side, and ignite, with a low
flame well at its base, until all the carbon of the filter has been
consumed. Allow the crucible to cool, add two drops of concentrated
nitric acid and one drop of concentrated hydrochloric acid, and heat
!very cautiously!, to avoid spattering, until the acids have been
expelled; then transfer the main portion of the precipitate from the
glazed paper to the cooled crucible, placing the latter on the larger
pi
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