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its close should be weighed so far as possible in a dry state. If wet the amount of moisture should be ascertained and allowed for, a sample being taken and dried for this purpose. This sample may serve also for analysis and the determination of unburned carbon and fusing temperature. The method above described for sampling coal may also be followed for obtaining a sample of the ashes and refuse. 12. CALORIFIC TESTS AND ANALYSES OF COAL The quality of the fuel should be determined by calorific tests and analysis of the coal sample above referred to.[70] 13. ANALYSES OF FLUE GASES For approximate determinations of the composition of the flue gases, the Orsat apparatus, or some modification thereof, should be employed. If momentary samples are obtained the analyses should be made as frequently as possible, say, every 15 to 30 minutes, depending on the skill of the operator, noting at the time the sample is drawn the furnace and firing conditions. If the sample drawn is a continuous one, the intervals may be made longer. 14. SMOKE OBSERVATIONS[71] In tests of bituminous coals requiring a determination of the amount of smoke produced, observations should be made regularly throughout the trial at intervals of 5 minutes (or if necessary every minute), noting at the same time the furnace and firing conditions. 15. CALCULATION OF RESULTS The methods to be followed in expressing and calculating those results which are not self-evident are explained as follows: (A) _Efficiency._ The "efficiency of boiler, furnace and grate" is the relation between the heat absorbed per pound of coal fired, and the calorific value of one pound of coal. The "efficiency of boiler and furnace" is the relation between the heat absorbed per pound of combustible burned, and the calorific value of one pound of combustible. This expression of efficiency furnishes a means for comparing one boiler and furnace with another, when the losses of unburned coal due to grates, cleanings, etc., are eliminated. The "combustible burned" is determined by subtracting from the weight of coal supplied to the boiler, the moisture in the coal, the weight of ash and unburned coal withdrawn from the furnace and ashpit, and the weight of dust, soot, and refuse, if any, withdrawn from the tubes, flues, and combustion chambers, including ash carried away in the gases,
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