FREE BOOKS

Author's List




PREV.   NEXT  
|<   8   9   10   11   12   13   14   15   16   17   18   19   20   21   22   23   24   25   26   27   28   29   30   31   32  
33   34   35   36   37   38   39   40   41   42   43   44   45   46   47   48   49   >>  
. The tube is next taken in both hands and held horizontally above the flame so that the scratch is exactly over it. The tubing is now rotated rapidly about its axis, and lowered so that the flame is just tangent to its lower side. After about ten seconds of heating, it is removed from the flame and the hot portion quickly breathed upon, when it will generally crack apart very nicely. Care must be taken to hold the tube at right angles to the flame during the heating, and to rotate it so that only a narrow strip of the circumference is heated, and the scratch should be in the center of this heated strip. By this means tubing as large as two inches in diameter is readily broken. Griffin's glass cutter, which contains a hardened steel wheel, like that on any ordinary window-glass cutter, and a device by which this can be made to make a true cut clear around the tube, is a very handy article, especially for large tubing, and may be obtained from any dealers in chemical apparatus. =Bending Glass.=--Inasmuch as this is one of the commonest operations in the laboratory, it is assumed that the reader knows how to perform it. However, it should be noted that in order to obtain the best results a broad (fish-tail burner) flame should generally be used, and the tube rotated on its axis during the heating, and allowed to bend mostly by its own weight. If large tubing is to be bent, one end must be stoppered and great care used. Whenever the tube shows signs of collapsing or becoming deformed, it must be gently blown out into shape, heating the desired spot locally if necessary. A blast-lamp is likely to be more useful here than the fish-tail burner. =Drawing Out a Tube.=--Most students learn this the first day of their laboratory work in chemistry, but few take pains to do it well. The tube should be heated in the flame of a Bunsen burner, or blast lamp (preferably the latter) until it is very soft. During this time it must be continuously rotated about its axis, and so held that the edges of the heated zone are sharply defined; _i.e._, it should not be allowed to move back and forth along its own axis. When so hot that it cannot longer be held in shape, the tube is removed from the flame, and the ends slowly and regularly drawn apart, _continuing the rotation of the tube about its axis_. By regulating the rate of drawing and the length of tube heated, the desired length and diameter of capillary may be obtained. The tube sh
PREV.   NEXT  
|<   8   9   10   11   12   13   14   15   16   17   18   19   20   21   22   23   24   25   26   27   28   29   30   31   32  
33   34   35   36   37   38   39   40   41   42   43   44   45   46   47   48   49   >>  



Top keywords:

heated

 

heating

 
tubing
 

rotated

 

burner

 

cutter

 

scratch

 

allowed

 

laboratory

 

obtained


desired
 
diameter
 
removed
 

generally

 

length

 

longer

 
slowly
 

locally

 

deformed

 

drawing


continuing
 

rotation

 

regulating

 

stoppered

 

regularly

 

collapsing

 

Whenever

 

gently

 

Drawing

 

Bunsen


weight
 

sharply

 

defined

 

preferably

 

During

 

continuously

 

capillary

 

students

 

chemistry

 

chemical


angles
 

nicely

 

rotate

 

inches

 

readily

 
broken
 

narrow

 

circumference

 

center

 

breathed