FREE BOOKS

Author's List




PREV.   NEXT  
|<   34   35   36   37   38   39   40   41   42   43   44   45   46   47   48   49   >>  
or by heating and drawing off the projections, and the new tube sealed on, usually with the first method (Exercise No. 1). If the break is very close to the stopcock, very little reheating and blowing can be done, on account of the danger of getting the stopcock sleeve out of shape, and the work must be heated very slowly to prevent cracking. The main reliance is then placed on making a good joint when the tubes are brought together, and then drawing out this joint a little, at once, to get an even wall. CLOSED CIRCUITS OF TUBING. In some pieces of apparatus closed circuits of circular or rectangular shape are required. A similar problem is involved in apparatus like the ordinary Soxhlet extractor, where a small tube is joined to the side of a large one, bent to form a siphon, and attached again to a continuation of the original large tube. The difficulty in all such cases is to provide for the contraction taking place as the last joint cools. If part of the circuit has the shape of the letter S, or is a spiral, the natural springiness of the glass will take care of this. If not, the side of the circuit opposite to the joint and parallel to it must be heated also, the two being finally heated together to the softening point after the joint is completed, and then allowed to cool together. To make the last joint, the rest of the tube is made in approximately the desired form, the two pieces which are to be joined to make the last joint being just enough out of the desired position to allow them to pass one another. The final joint is preferably made in the middle of a straight piece of tube, not at a tee. The two pieces which are to be joined are bent so as to just pass each other, marked at the right point with the glass-knife, and cut there, preferably with a small bead of hot glass. One or both of these tubes are now warmed to the softening point in such a place that the tubes can be made to meet properly, and the two cut ends pressed together. They are now warmed in the flame, and joined together, either by simultaneously warming the opposite side of the circuit or some other suitable part, so as to allow the two ends to be pushed together again after they are softened, or by gently touching the places that do not unite with a hot bead of glass, and using the glass to fill up the crack where the ends do not quite meet. Care must be taken not to leave knots or lumps of glass in the finished joint, and the latt
PREV.   NEXT  
|<   34   35   36   37   38   39   40   41   42   43   44   45   46   47   48   49   >>  



Top keywords:

joined

 

heated

 
circuit
 

pieces

 

preferably

 

apparatus

 

desired

 

opposite

 

softening

 

stopcock


warmed
 
drawing
 
approximately
 

places

 

allowed

 

finally

 
finished
 

position

 

completed

 

straight


properly
 

middle

 

marked

 

pressed

 

pushed

 

softened

 

gently

 

suitable

 

warming

 

simultaneously


touching
 

difficulty

 

reliance

 

cracking

 

prevent

 

sleeve

 

slowly

 

making

 

CLOSED

 

brought


danger
 

method

 

sealed

 

heating

 

projections

 
Exercise
 

blowing

 

account

 

reheating

 

CIRCUITS