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ce four dots on the filter, two each on diameters which are at right angles to each other. Then proceed as follows: (1) Fold the filter evenly across one of the diameters, creasing it carefully; (2) open the paper, turn it over, rotate it 90 deg. to the right, bring the edges together and crease along the other diameter; (3) open, and rotate 45 deg. to the right, bring edges together, and crease evenly; (4) open, and rotate 90 deg. to the right, and crease evenly; (5) open, turn the filter over, rotate 22-(1/2) deg. to the right, and crease evenly; (6) open, rotate 45 deg. to the right and crease evenly; (7) open, rotate 45 deg. to the right and crease evenly; (8) open, rotate 45 deg. to the right and crease evenly; (9) open the filter, and, starting with one of the dots between thumb and forefinger of the right hand, fold the second crease to the left over on it, and do the same with each of the other dots. Place it, thus folded, in the funnel, moisten it, and fit to the side of the funnel. The filter will then have four short segments where there are three thicknesses and four where there is one thickness, but the latter are evenly distributed around its circumference, thus greatly aiding the passage of liquids through the paper and hastening both filtration and washing of the whole contents of the filter. !SAMPLE PAGES FOR LABORATORY RECORDS! !Page A! Date CALIBRATION OF BURETTE No. ___________________________________________________________________________ | | | | BURETTE | DIFFERENCE | OBSERVED | DIFFERENCE | CALCULATED READINGS | | WEIGHTS | | CORRECTION _______________|______________|______________|______________|______________ 0.02 | | 16.27 | | 10.12 | 10.10 | 26.35 | 10.08 | -.02 20.09 | 9.97 | 36.26 | 9.91 | -.06 30.16 | 10.07 | 46.34 | 10.08 | +.01 40.19 | 10.03 | 56.31 | 9.97 | -.06 50.00 | 9.81 | 66.17 | 9.86 | +.05 _______________|______________|______________|______________|______________ These data to be obtained in duplicate for each burette. !Page B! Date DETERMINATION OF COMPARATIVE STRENGTH HCl vs. NaOH ________________________________________
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