FREE BOOKS

Author's List




PREV.   NEXT  
|<   238   239   240   241   242   243   244   245   246   247   248   249   250   251   252   253   254   255   256   257   258   259   260   261   262  
263   264   265   266   267   268   269   270   271   272   273   274   275   276   277   278   279   280   281   282   283   284   285   286   287   >>   >|  
two or more tubes, which frequently happens when we have not a sufficient number of bottles with two or three necks, we must use a cork with two or three holes, Pl. IV. Fig. 8. When the whole apparatus is thus solidly joined, so that no part can play upon another, we begin to lute. The lute is softened by kneading and rolling it between the fingers, with the assistance of heat, if necessary. It is rolled into little cylindrical pieces, and applied to the junctures, taking great care to make it apply close, and adhere firmly, in every part; a second roll is applied over the first, so as to pass it on each side, and so on till each juncture be sufficiently covered; after this, the slips of bladder, or of linen, as above directed, must be carefully applied over all. Though this operation may appear extremely simple, yet it requires peculiar delicacy and management; great care must be taken not to disturb one juncture whilst luting another, and more especially when applying the fillets and ligatures. Before beginning any experiment, the closeness of the luting ought always to be previously tried, either by slightly heating the retort A, Pl. IV. Fig. 1, or by blowing in a little air by some of the perpendicular tubes S s s s; the alteration of pressure causes a change in the level of the liquid in these tubes. If the apparatus be accurately luted, this alteration of level will be permanent; whereas, if there be the smallest, opening in any of the junctures, the liquid will very soon recover its former level. It must always be remembered, that the whole success of experiments in modern chemistry depends upon the exactness of this operation, which therefore requires the utmost patience, and most attentive accuracy. It would be of infinite service to enable chemists, especially those who are engaged in pneumatic processes, to dispense with the use of lutes, or at least to diminish the number necessary in complicated instruments. I once thought of having my apparatus constructed so as to unite in all its parts by fitting with emery, in the way of bottles with cristal stoppers; but the execution of this plan was extremely difficult. I have since thought it preferable to substitute columns of a few lines of mercury in place of lutes, and have got an apparatus constructed upon this principle, which appears capable of very convenient application in a great number of circumstances. It consists of a double necked bottle A, Pl.
PREV.   NEXT  
|<   238   239   240   241   242   243   244   245   246   247   248   249   250   251   252   253   254   255   256   257   258   259   260   261   262  
263   264   265   266   267   268   269   270   271   272   273   274   275   276   277   278   279   280   281   282   283   284   285   286   287   >>   >|  



Top keywords:

apparatus

 

applied

 

number

 

juncture

 

constructed

 

junctures

 

liquid

 

luting

 

requires

 

extremely


operation

 

thought

 

alteration

 
bottles
 

enable

 

infinite

 
accuracy
 
attentive
 

service

 

chemists


success

 

smallest

 
opening
 

permanent

 

accurately

 

recover

 

depends

 

exactness

 

utmost

 

chemistry


modern

 

remembered

 

experiments

 

patience

 

fitting

 

mercury

 

columns

 

difficult

 

preferable

 

substitute


principle

 

consists

 

double

 
necked
 

bottle

 

circumstances

 

application

 

appears

 
capable
 
convenient