FREE BOOKS

Author's List




PREV.   NEXT  
|<   9   10   11   12   13   14   15   16   17   18   19   20   21   22   23   24   25   26   27   28   29   30   31   32   33  
34   35   36   37   38   39   40   41   >>  
is sufficient to melt copper. When taken out, it weighed three drams and one scruple, or had lost 7/12 of its former weight. I repeated, with the _magnesia_ prepared in this manner, most of those experiments I had already made upon it before calcination, and the result was as follows. It dissolves in all the acids, and with these composes salts exactly similar to those described in the first set of experiments: but what is particularly to be remarked, it is dissolved without any the least degree of effervescence. It slowly precipitates the corrosive sublimate of mercury in the form of a black powder. It separates the volatile alkali in salt ammoniac from the acid, when it is mixed with a warm solution of that salt. But it does not separate an acid from a calcarious earth, nor does it induce the least change upon lime-water. Lastly, when a dram of it is digested with an ounce of water in a bottle for some hours, it does not make any the least change in the water. The _magnesia_, when dried, is found to have gained ten grains; but it neither effervesces with acids, nor does it sensibly affect lime-water. Observing _magnesia_ to lose such a remarkable proportion of its weight in the fire, my next attempts were directed to the investigation of this volatile part, and, among other experiments, the following seemed to throw some light upon it. Three ounces of _magnesia_ were distilled in a glass retort and receiver, the fire being gradually increased until the _magnesia_ was obscurely red hot. When all was cool, I found only five drams of a whitish water in the receiver, which had a faint smell of the spirit of hartshorn, gave a green colour to the juice of violets, and rendered the solutions of corrosive sublimate and of silver very slightly turbid. But it did not sensibly effervesce with acids. The _magnesia_, when taken out of the retort, weighed an ounce, three drams, and thirty grains, or had lost more than the half of its weight. It still effervesced pretty briskly with acids, tho' not so strongly as before this operation. The fire should have been raised here to the degree requisite for the perfect calcination of _magnesia_. But even from this imperfect experiment, it is evident, that of the volatile parts contained in that powder, a small proportion only is water; the rest cannot, it seems, be retained in vessels, under a visible form. Chemists have often observed, in their distillations, that par
PREV.   NEXT  
|<   9   10   11   12   13   14   15   16   17   18   19   20   21   22   23   24   25   26   27   28   29   30   31   32   33  
34   35   36   37   38   39   40   41   >>  



Top keywords:
magnesia
 

experiments

 

volatile

 
weight
 

change

 

sublimate

 

powder

 

grains

 
corrosive
 
degree

receiver

 

calcination

 

retort

 

proportion

 

weighed

 

sensibly

 

violets

 

ounces

 

rendered

 
gradually

solutions
 

distilled

 
obscurely
 

silver

 

hartshorn

 

whitish

 

spirit

 
increased
 
colour
 

pretty


contained
 

evident

 

imperfect

 

experiment

 

retained

 

observed

 

distillations

 

Chemists

 

vessels

 

visible


perfect

 

requisite

 

thirty

 
effervesce
 

slightly

 

turbid

 

effervesced

 

raised

 

operation

 

strongly