been filled with water, the latter flows into
the next by means of a small pipe attached to it. In order to expose a
large surface to the vapors, the condensing trough is fitted internally
with a number of vertical partitions, which are open at alternate ends, so
that the vapors may travel along the partitions in the trough from one end
to the other. The boiler is filled with water, and 120 kilogrammes of
chopped pieces of wood are introduced into the tub, which is then closed
with a cover, cemented with clay, so as to make it air-tight. Firing is
then begun; the steam passes into the tub, and thus carries the vapors of
camphor and oil into the condenser, in which the camphor solidifies, and
is mixed with the oil and condensed water. After twenty-four hours the
charge is taken out from the tub, and new pieces of the wood are
introduced, and distillation is conducted as before. The water in the
boiler must be supplied from time to time. The exhausted wood is dried and
used as fuel. The camphor and oil accumulated in the trough are taken out
in five or ten days, and they are separated from each other by filtration.
The yield of the camphor and oil varies greatly in different seasons. Thus
much more solid camphor is obtained in winter than in summer, while the
reverse is the case with the oil. In summer, from 120 kilogrammes of the
wood 2.4 kilogrammes, or 2 per cent. of the solid camphor are obtained in
one day, while in winter, from the same amount of the wood, 3 kilogrammes,
or 2.5 per cent., of camphor are obtainable at the same time.
The amount of the oil obtained in ten days, _i.e._, from 10 charges or
1,200 kilogrammes of the wood, in summer is about 18 liters, while in
winter it amounts only to 5-7 liters. The price of the solid camphor is
at present about 1s. 1d. per kilo.
The oil contains a considerable amount of camphor in solution, which is
separated by a simple distillation and cooling. By this means about 20 per
cent. of the camphor can be obtained from the oil. The author subjected the
original oil to fractioned distillation, and examined different fractions
separately. That part of the oil which distilled between 180 deg.-185 deg. O. was
analyzed after repeated distillations. The following is the result:
Found. Calculated as
C_{10}H_{16}O.
C = 78.87 78.95
H = 10.73 10.52
O = 10.40 (by difference) 10.52
The co
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